Introduction to Microwave Sample Preparation: Theory and Practice
Howard M. Kingston, L. B. Jassie
American Chemical Society, 1988 - Science - 263 pages
Provides a theoretical basis for understanding microwave acid sampling requiring elemental or chemical analysis. Describes techniques and equipment found most effective. Gives direct practical applications of the methods to a variety of sample types. Covers most aspects of closed vessel microwave digestion and open vessel acid composition. Demonstrates fundamental relationships that can be used to predict the conditions that will occur under specific parameter settings. Addresses safety considerations for each technique demonstrated. This book is truly multidisciplinary--its techniques can be used in inorganic elemental analysis, sample digestion, food analysis, environmental sample preparation chemistry, and other areas.
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Theoretical Concepts and Equipment Design
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absorbed acid decomposition acid digestion acid dissolution acid mixture American Chemical Society Anal analysis Analytical Chemistry aqua regia automated aztreonam biological boiling point Caro's acid CEM Corporation Chem closed-vessel concentration container cooling crowave dielectric relaxation digestion method digestion vessel dilution dipole rotation dissipation factor dissolve elements equipment Figure flask glass HNO3 hydrochloric acid hydrofluoric acid increase instruments Jassie Kingston Kjeldahl digestion Kjeldahl method laboratory magnetron matrix measurement metal microwave acid microwave cavity microwave digestion system microwave dissolution microwave energy microwave Kjeldahl microwave oven microwave power microwave system microwave unit mineral acids monitoring nitric acid nitrogen open-vessel operation oxidizing perchloric acid power absorption predict predigestion present pressure dissolution pressure profile probe procedure reaction vessel reagents robot safety sample preparation selenium Standard Reference Materials sulfuric acid Table technique Teflon PFA vessels Teflon vessels temperature and pressure tube turntable valve